ONS-ACI.png




List of all experiments


NOTE: All solubility experiments by the Bradley group past this point are recorded on the ONS challenge wiki.

EXP286 Synthesis of aldol condensation product of phenanthrene-9-carboxaldehyde and acetone in methanol using NaOH as the catalyst. -Matthew McBride
EXP285 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - Matthew McBride
EXP284 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - Matthew McBride
EXP283 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - Matthew McBride
EXP282 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as catalyst. - Matthew McBride
EXP281 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - Matthew McBride
Exp280 Synthesis of benzalaniline in ethanol to prepare enough for solubility studies.
Exp279 Synthesis of benzalaniline in ethanol to test the effect of the ratio of aldehyde to amine- Mark
Exp278 Synthesis of benzalaniline in ethanol to test the effect of the ratio of aldehyde to amine- Mark
Exp277 Synthesis of Benzalaniline in Methanol at 0.2M to test kinetic reaction rate- Mark
Exp276 Synthesis of benzalaniline in ethanol at 0.2M and to test amine effect of concentrations - Mark
Exp275 Observing the hydrolysis of benzalaniline in 90/10(vol) methanol/water solution - Evan
Exp274 Synthesis of benzalaniline in methanol at 2M and recrystallization in ethanol to test yield predictions - Evan
Exp273 Observing the hydrolysis of benzalaniline in 90/10(vol) ethanol/water solution - Evan
Exp272 Determination of the melting point of cyclobutylamine - Evan
Exp271 Synthesis of benzalaniline in trifluoroethanol, n-hexane and isopropanol - Evan
Exp270 Recovery of benzalaniline from ONSexp213 - Evan
Exp269 Synthesis of 3 imines from salicylaldehyde, 4-(dimethylamino)benzaldehyde and p-anisaldehyde with aniline. - Evan
Exp268 Synthesis of an imine from vanillin and aniline - Evan
Exp267 Determination of the melting point of benzylamine JCB
Exp266 Determination of the melting point of 4-benzyltoluene - Evan
Exp265 Determination of the melting point of benzylamine - Evan
Exp264 Synthesis of Ugi 233 and Ugi 234 Repeat - David
Exp263 Synthesis of benzalaniline at 2M concentration in ethanol - Evan
Exp262 Synthesis of four imines from vanillin, p-chlorobenzaldehyde, aniline and o-chloroaniline - Evan
Exp261 Synthesis of an imine from benzaldehyde and aniline - Evan
Exp260 Synthesis of Ugi products from formaldehyde, methylamine, formic acid and n-butylisocyanide and t-butylisocyanide in methanol- Khalid
Exp259 Ugi synthesis of UCExp064C - Khalid
Exp258 Ugi synthesis of the precursor of praziquantel - Khalid
Exp257 Synthesis of UC176C in ethyl acetate - Khalid
Exp256 Synthesis of UC176C in benzene - Khalid
Exp255 Synthesis of UC176C in methanol and benzene - Khalid
Exp254 Kinetic study for the formation UC176C in methanol via a Ugi reaction - Khalid
Exp253 Synthesis of three Ugi products UC176C in methanol - Khalid
Exp252 Kinetic study of Ugi reaction for the formation of UC176C in benzene - Khalid
Exp251 Synthesis of three Ugi products , UC176C, 148C and 150D - Khalid
Exp250 Synthesis of a Ugi product in benzene - Khalid
Exp249 Kinetic study of Ugi reaction in benzene - Khalid
Exp248 Synthesis of methyl ester of L-tryptophan- Khalid
Exp247 Synthesis of 10 Ugi products in THF - Khalid
Exp246 Kinetic study of Ugi reaction in benzene - Khalid
Exp245 Synthesis of top 20 Ugi products in methanol - Khalid
Exp244 Synthesis of 2 Ugi products in benzene - Marshall Moritz
Exp243 Oxidation of 1-phenylethanol with NaH -Khalid, Marshall
Exp242 Synthesis of 10 Ugi products in benzene with phenanthrene-9-carboxaldehyde - Marshall Moritz
Exp241 Ugi synthesis of 38 Ugi products in methanol - Khalid
Exp240 Ugi synthesis of 12 Ugi products in THF with phenanthrene-9-carboxaldehyde - Khalid
Exp239 Synthesis of a Ugi product in benzene with phenanthrene-9-carboxaldehyde - Marshall Moritz
Exp238 Ugi synthesis of 44 Ugi products in THF with phenanthrene-9-carboxaldehyde as aldehyde component - Khalid, Cedric
Exp237 Ugi synthesis of a Ugi product in methanol and THF with phenanthrene-9-carboxaldehyde - Khalid
Exp236 Ugi synthesis of 28 Ugi products in methanol - Khalid
Exp235 Ugi synthesis of two Ugi products in methanol - Khalid, Jenna
Exp234 Ugi synthesis of ten Ugi products in methanol (Ugi Reaction Blog#002) - David
Exp233 Ugi synthesis of six Ugi products in methanol (Ugi Reaction Blog#001) - David
Exp232 Ugi synthesis of 75 Ugi products in methanol - Khalid
Exp231 Ugi synthesis of nine Ugi products from the top 20 list of Sortase inhibitors - Khalid
Exp230 Ugi synthesis of four Ugi products in eight solvents at three concentrations - David
Exp229 Ugi synthesis of two new Ugi products in methanol - David
Exp228 Ugi synthesis of seven Ugi products six of them were in the top 20 list of Sortase inhibitors - Khalid
Exp227 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid - Khalid
Exp226 Ugi synthesis of eight Ugi products with1-pyrenebutyric acid - David
Exp225 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- Khalid
Exp224 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- Khalid
Exp223 Ugi synthesis of previously made 62E - David
Exp222 Effect of solvent and conc on few Ugi reactions- Khalid
Exp221 Effect of solvent and conc on few Ugi reactions - Khalid
Exp220 Effect of solvent and conc on few Ugi reactions - Khalid
Exp219 Three Ugi reactions involving 4-pyrenebutanoic acid in a bisolvent system (methanol/THF) - Khalid
Exp218 To test if deuterated methanol, acetone, chloroform and benzene can be distinguished by smell - Khalid
Exp217 Effect of THF as solvent on for 4 Ugi reaction, Effect of DMSO as a solvent on a Ugi reaction. - Khalid
Exp216 Ugi synthesis of ten previously made and three new Ugi products. - Khalid
Exp215 Ugi synthesis of nine Ugi products. - Khalid
Exp214 Ugi synthesis of previously made 150D using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butylisocyanide - Khalid
Exp213 Solubility of 4-chlorobenzaldehyde in chloroform and methanol by UV spectroscopy - Khalid
EXP212 Solubility measurements of p-nitrobenzaldehyde in different solvents. Tim
EXP211 Solubility estimation by UV-VIS Khalid
EXP210 Solubility estimation in methanol and ethanol Khalid
EXP209 Determination of the time parameter for chloroform containing solutions in speedvac. Khalid/Tim
EXP208 Solubility measurements of 9 aldehydes in 6 different solvents. Khalid/Tim
EXP207 Solubility measurements of boc-gly, vanillin and other compounds in methanol, ethanol and THF JCB
Exp206 Purification of the ugi product - Khalid
Exp205 Solubilities of 10 aldehydes in methanol -Tim and Khalid
Exp204 Determination of solubility of Ugi adduct (99C) in Methanol, Ethanol, Acetonitrile, Tetrahydrofuran, Acetone, Hexane, Chloroform, and Distilled Water - Cedric and Aneta
Exp203 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp202 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp201 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp200 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide (verified by TomO) - Khalid
Exp199 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide (verified by TomO) - Khalid
Exp198 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp197 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp196 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp195 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp194 missing
Exp193 missing
Exp192 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp191 Repeat of Exp189 - Khalid
Exp190 42 Ugi reactions on Minimapper -Trial 2 - Khalid
Exp189 Ugi reaction optimization using MiniMapper - Trial 1 - Khalid
Exp188 Ugi synthesis- Effect of Concentration - Khalid
Exp187Ugi synthesis- Effect of Concentration - Khalid
Exp186 Ugi synthesis (V2 Rank 83) using benzaldehyde, aniline, 1-pyrenebutyric acid and n-butylisocyanide-Emily
Exp185 Ugi synthesis- Effect of Concentration - Khalid
Exp184 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- Emily
Exp183 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- Emily
Exp182 Ugi synthesis (V1 Rank 28) using heptylamine, phenanthrene-9-carboxaldehyde, furoic acid and n-butyl isocyanide- Emily
Exp181 Synthesis of compounds ranked 55-124 from library DEXP014-V2B Khalid
Exp180 Ugi synthesis (V1 Rank 40) using heptylamine, phenanthrene-9-carboxaldehyde, acetic acid and n-butyl isocyanide- Shannon
Exp179 Ugi synthesis (V1 Rank 44) using aniline, phenanthrene-9-carboxaldehyde, 4-chlorophenyl acetic acid and t-butyl isocyanide- Shannon
Exp178 Ugi synthesis (V1 Rank 29) using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Shannon
Exp177 Ugi synthesis (V1 Rank 38) using propylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Shannon
Exp176 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily/ Khalid
Exp175 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- Emily/Khalid
Exp174 Synthesis of compounds ranked 31-54 (except 32,37) from library DEXP014-V2B Khalid
Exp173 Synthesis of compounds ranked 13-29 (except 23) from library DEXP014-V2B Khalid
Exp172 (aborted) Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-Lauren/Tim (repeat of Exp168)
Exp171 Synthesis of compounds ranked 1-12 from library DEXP014-V2B Khalid
Exp170 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily
Exp169 !! Ugi synthesis using phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid, cyclohexylamine, and t-butyl isocyanide.-Tim
Exp168 !! Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-Tim
Exp167-!! Ugi synthesis using propylamine, phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid and n-butyl isocyanide- Tim.
Exp166 !! Plasmodium falciparum inhibition results for 2 Ugi products Jiri
Exp165 !! Falcipain-2 inhibition results for 2 Ugi products Jiri
Exp164 Ugi synthesis using aniline, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily/Shannon
Exp163 !! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- Tim (repeat of Exp161)
Exp162 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide (Repeat of Exp157)- Shannon
Exp161-!! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- Tim
Exp160 !! synthesis using phenanthrene-9-carboxaldehyde, furfurylamine, 3,4-dihydroxyphenyl acetic acid and n-butyl isocyanide- Emily
Exp159 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- Emily
Exp158 Ugi synthesis using 4-chlorobenzaldehyde, 5-methylfurfurylamine, salicylic acid and tosylmethyl isocyanide- Emily
Exp157 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide- Shannon
Exp156 Ugi synthesis using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butyl isocyanide- Emily
Exp155 Ugi synthesis using benzaldehyde, 5-methyl-2-furylmethylamine, 3-(4-methoxyphenyl) propanioc acid, and t-butyl isocyanide- Tim/Emily
Exp154 Three attempts of Ugi synthesis- Shannon
Exp153 One attempt of Ugi synthesis -Mitesh
Exp151 One attempt of Ugi synthesis- Mitesh
Exp150 Ugi synthesis with Benzylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and tert-butyl isocyanide- Emily / Khalid
Exp149 ugi synthesis using phenanthrene -9- carboxaldehyde, hexylamine, benzoic acid and n-butylisocyanide., Aneh/ Khalid
Exp148 Ugi synthesis with Heptylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and tert-butyl isonitrile - Emily / Khalid
Exp147 Four attempts of Ugi synthesis - Mitesh/Rikesh
Exp146 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp144 Three attempts of Ugi synthesis - Rikesh/Mitesh
Exp143 Five attempts of Ugi synthesis - Emily
Exp142 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp141 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp140 Two attempts of Ugi synthesis - Emily/ Khalid
Exp139 Ten attempts of Ugi synthesis-aneh
Exp138 Three attempts of Ugi synthesis - Shannon
Exp137 Eight attempts of Ugi synthesis - Anett, Rikesh, Mitesh, Khalid
Exp136 Ugi synthesis using o-vanillin, benzylamine, Boc-Trp-OH, and n-pentylisocyanide - Mitesh/Rikesh
Exp135 Ugi synthesis using o-vanillin, hexylamine, Boc-Trp-OH, and benzyl isocyanide - Rikesh
Exp134 Four attempts of Ugi synthesis - Rikesh
Exp133 Synthesis of N-benzyl-N-(2-furylmethyl)acetamide - Khalid
Exp132 Synthesis of N-benzyl-N-[(5-methyl-2-furyl)methyl]acetamide - Khalid
Exp131 Nine Attempts of Ugi synthesis - Rikesh
Exp130 Five Attempts of Ugi synthesis - Rikesh
Exp129 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - Jessica/ Khalid
Exp128 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - Jessica/ Khalid
Exp127 Test for the stability of the furan ring of 109C Ugi adduct in TFA - Jessica/ Khalid
Exp126 Five attempts of Ugi synthesis - Jessica
Exp125 Three attempts of Ugi synthesis - Jessica
Exp124 Two attempts of Ugi synthesis - Khalid
Exp123 Ugi synthesis using furfuylamine, o-vanillin, Boc-Tryptophan, and n-butyl isocyanide - Jessica
Exp122 Ugi synthesis using methylamine, o-tolualdehyde, acetic acid, and p-toluenesulfonylmethyl isocyanide - Jessica
Exp121 Ugi synthesis using o-Vanillin, 5-methyl furfurylamine Boc-tryptophan and 1-pentylisocyanide- Khalid
Exp120 Ugi synthesis using o-Vanillin, furfurylamine Boc-tryptophan and 1-pentylisocyanide- Khalid
Exp119 Two attempts of Ugi synthesis - Jessica/ Khalid
Exp118 Purify propionaldehyde by distillation - Khalid
Exp117 Monitor Ugi synthesis using propionaldehyde, methylamine, acetic acid and tert-butyl isocyanide by NMR - Khalid
Exp116 Four attempts of Ugi synthesis - Khalid
Exp115 Monitor Ugi synthesis using furfural, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid by NMR - Khalid
Exp114 Ugi synthesis using furfuraldehyde, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid - Khalid
Exp113 Ugi synthesis using Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, and Boc-glycine - Jessica/ Khalid
Exp112 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid / Jessica
Exp111 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid / Jessica
Exp110 Reaction of the Ugi product 108C with 50% TFA in CDCl3 (prolonged exposure) - Khalid / Jessica
Exp109 Ugi synthesis using 5-(Trifluoromethyl)-2-furylmethylamine, benzaldehyde, benzylisocyanide and boc-glycine - Khalid
Exp108 Ugi synthesis using furfurylamine, benzaldehyde, benzylisocyanide and boc-glycine - Khalid
Exp107 Tert-butylation of furfurylamine with t-butanol and Amberlyst 15(H) in CDCl3 at room temperature - Khalid
Exp106 Ugi synthesis using 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide and Boc-Gly-OH - Sean
Exp105 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide-Khalid
Exp104 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp103 Synthesis of the acetamide of furfurylamine -Khalid
Exp102 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide-Khalid
Exp101 Reaction of the Ugi product 99C with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp100 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp099 Ugi synthesis using furfurylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp098 Reaction of the Ugi product 64C with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp097 Reaction of the Ugi product 86B with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp096 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp095 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp094 3,4-Dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Glycine, t-Butyl isocyanide (CHCl3 for imine, MeOH for rxn) - Sean
Exp093 Ugi synthesis using aniline, benzophenone, tert-butylisocyanide and boc-glycine - Khalid
Exp092 Test for the stability of the furan ring of amide of BocGlycine and 5MFA in 50% TFA - Khalid
Exp091 Reaction of the Ugi product 62E with 50% TFA in CDCl3. - Khalid
Exp090 Reaction of the Ugi product 62E with 10% TFA in CDCl3 - Alicia
Exp089 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp088 Synthesis of an amide of Boc Glycine and 5-methylfurfurylamine in methanol-d4- Khalid
*Exp087 Synthesis of the Boc-deprotected amine of the Ugi product 86C- Khalid
Exp086 Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, Boc-glycine - Khalid
Exp085Crotonaldehyde, Methylfurfurylamine in CDCl3 - jgiammarco
Exp084Piperonal, Aniline, Boc-Gly-OH, Tertbutyalisocyanide in CDCl3- jgiammarco
Exp083Crotonaldehyde, Tertbutyalamine, Boc-Gly-OH, Tertbutylisocyanide in CDCl3- jgiammarco
Exp082 Synthesis of the Boc-deprotected amine of the Ugi product(64C-2) - Khalid
Exp081 Test for the stability of the furan ring of N-[(5-methyl-2-furyl)methyl]acetamide in 10% TFA - Khalid
Exp080 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutylisocyanide (CDCl3) -jgiammarco
Exp079 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Alicia
Exp078 Synthesis of the acetamide of 5-methyl furfurylamine -Khalid
Exp077 Piperonal, tertbutylamine, Boc-Gly-OH(CDCl3) -jgiammarco
Exp076 Piperonal, tertbutylamine, Boc-Gly-OH (MeOH) -jgiammarco
Exp075 Perform a MALDI MS analysis of the Ugi product 62E - kgowens
Exp074 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - Khalid
Exp073 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid
Exp072 Ugi Product (diamide) Cycliztion using 10% HCl in CDCl3 - Alicia
Exp071 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - Khalid
Exp070 Ugi Product (diamide) Cycliztion using 50% TFA in CDCl3 - Khalid
Exp069 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
Exp068 Reaction of Boc-Glycine with 10%TFA in CDCl3 - Khalid
Exp067 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Khalid
Exp066 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
*Exp065 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Alicia
*Exp064 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH - Khalid
*Exp063 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, benzyl isocyanide - Sean
*Exp062 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - Alicia
*Exp061 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, t-butyl isocyanide - Sean
*Exp060 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH- Khalid
*Exp059 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - Alicia
Exp058 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
Exp057 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - Sean
Exp056 Boc-Met-OH and 5-Methyl furfurylamine in MeOH-d4 - Khalid
Exp055 Boc-Gly-OH and 5-Methyl furfurylamine in MeOH-d4 - Khalid
Exp054 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide and final addition of Boc-Gly-OH in MeOH-d4 - Khalid
Exp053 Boc-Gly-OH and tert-butyl isocyanide in MeOH-d4 - Khalid
*Exp052 Piperonal, 5-methylfurfurylamine, BocGly-OH, tert-butyl isocyanide in MeOH - Alicia
Exp051 Piperonal and tert-butylamine, Boc-Gly-OH and dehydration with MgSO4 in MeOH-d4 - jgiammarco
Exp050 Boc-Gly-OH and Benzyl isocyanide in MeOH-d4 - Khalid
Exp049 Boc-Gly-OH and 2-morpholinoethyl isocyanide in MeOH-d4 - Khalid
Exp048 (piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH-d4) - jgiammarco
Exp047 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - Sean
Exp046 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in MeOH-d4) - Khalid
*Exp045 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) - Khalid
Exp044 Formation of the imine of Phenyl acetaldehyde and tert-butylamine in CDCl3- Khalid
Exp043 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4 - Alicia
Exp042 Formation of the imine of Phenyl acetaldehyde and tert-butylamine in CDCl3- Khalid / Lin
Exp041 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4- Alicia
Exp040 Formation of the imine of Piperonal and 5-Methyl furfurylamine in CDCl3- Alicia
Exp039 Distillation of Phenylacetaldehyde (39B pure) - Khalid / Lin
Exp038 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3 ) - Alicia
Exp037 Distillation of Phenylacetaldehyde (contaminated)- jgiammarco
Exp036 Preparation of N-tert-butylphenylacetaldimine (impure by HMR)- Khalid
Exp035 Distillation of Phenylacetaldehyde(impure by HMR) - Khalid
Exp034 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) - Alicia
Exp033 Distillation of Butyraldehyde (impure by HMR) - Alicia
Exp032 (Imine mix from Exp036, Boc-Met-OH, 2-morpholinoethylisocyanide in MeOH ) - Khalid
Exp031 (Phenylacetaldehyde after distillation, -methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) - jgiammarco
Exp030 (Piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH) - Khalid
Exp029 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH then CDCl3) - Alicia
Exp028 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in 1M LiCl/Water) - Khalid
Exp027 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in Methanol) - Khalid
Exp026 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) Lin
EXP025 Convert adrenaline to DOPAL by acid catalysis - (2006-08-31) Khalid/Lin (pure without chromatography)
EXP024 Convert adrenaline to DOPAL by acid catalysis - Khalid/Lin
EXP023 (DOPAL, 5-methylfurfurylamine, N-(tert)-butoxycarbonyl)-L-methionine, and benzylisocyanide) - Khalid (crude)
EXP022 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) Khalid
EXP021 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) jgiammarco
EXP020 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) jgiammarco
EXP019 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) - Lin
EXP018 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) jgiammarco
EXP017 (Piperonal, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) - Lin
EXP016 Convert adrenaline to DOPAL using phosphoric acid - jgiammarco
EXP015 Convert adrenaline to DOPAL using phosphoric acid - jgiammarco
EXP014 (Phenylacetaldehyde, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) - Khalid
EXP013 Convert adrenaline to a catechol aldehyde using CH3COOH- jgiammarco
EXP012 Convert adrenaline to a catechol aldehyde using H2SO4- jgiammarco
EXP011 Convert adrenaline to a catechol aldehyde using H2SO4 and a benzene layer- jgiammarco
EXP010 Convert adrenaline to a catechol aldehyde using H2SO4 - jgiammarco
EXP009 Convert adrenaline to a catechol aldehyde using H2SO4, benzene, and water - jgiammarco
EXP008 Convert adrenaline to a catechol aldehyde using H2SO4 and benzene - jgiammarco
EXP007 Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - Alicia
EXP006 (Phenylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) - Khalid
EXP005 Synthesis of 3,4-dihydroxyphenylacetaldehyde from adrenaline -jgiammarco
EXP004 Convert adrenaline to a catechol aldehyde using CH3COOH, H2SO4, and water - Brett
EXP003 (Phehylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) - Brett/Alicia/jgiammarco
EXP002 Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - jgiammarco
EXP001 Convert adrenaline to a catechol aldehyde using MeOH - Jean-Claude Bradley

Usefulchem Table of Chemicals