Exp145

== =Objective= To synthesize 1 Ugi product following the EXPLAN005. = = =Procedure= As described in Explan005. This is a repeat of Exp130-4
 * **Comp ID**/ **Lib Rank** || **Methanol Added** || **Aldehyde** || **Amine** || **Carboxylic Acid** || **Isocyanide** || **Ppt Yes/No** ||
 * 130-4 || 500uL || B-napthaldehyde (0.53mmol, 82.8mg) || furfurylamine (0.53mmol, 46.8uL) || formic acid (0.53mmol, 20.0uL) || benzylisocyanide (0.53mmol, 64.4uL) ||  ||

=Results=

=Discussion=

=Conclusion=

=Log=

2007-11-14
11:45 Weighed B-naphthaldehyde(0.53mmol,82.8mg) 11:55 Added 500 uL of Methanol to one dram vial. 12:00 Added furfurylamine (0.53mmol, 46.8uL), vortexed solution for 15 seconds. 12:02 Added B-napthaldehyde (0.53mmol, 82.8mg) and vortexed solution for 15 seconds. 12:04 Added formic acid (0.53mmol, 20.0uL) and vortexed solution for 15 seconds. 12:06 Added benzylisocyanide (0.53mmol, 64.4uL) and vortexed solution for 15 seconds.\ 12:13 Took picture of solution after all reagents were combined.

=Tags=

[|benzylisocyanide] [|InChI=1/C8H7N/c1-9-7-8-5-3-2-4-6-8/h2-6H,7H2] [|B-naphthaldehyde] [|InChI=1/C11H8O/c12-8-9-5-6-10-3-1-2-4-11(10)7-9/h1-8H] [|formic acid] [|InChI=1/CH2O2/c2-1-3/h1H,(H,2,3)] [|furfurylamine] [|InChI=1/C5H7NO/c6-4-5-2-1-3-7-5/h1-3H,4,6H2]