Exp278

=Researchers= Mark Mangir Stephanie Costa

=Results=
 * [|Mass and Yield Calculations]**


 * [|NMR for the Samples]**

=Log=

2012-02-27
 12:13- 1.2440g of 4-chlorobenzaldehyde was placed into test tube 1  12:22- 0.6219g of 4-chlorobenzaldehyde was placed into test tube 2  12:24- 0.6195g of 4-chlorobenzaldehyde was placed into test tube 3  12:26- 0.4202g Aniline was placed into vial 1  12:27- 0.4258g Aniline was placed into vial 2  12:28- 0.8435g Aniline was placed into vial 3  12:33- using a 10mL graduated cylinder, 10mL ethanol was measured out and added to test tube 1, which was then inverted several times  12:35- using a 10mL graduated cylinder, 10mL ethanol was measured out and added to test tube 2, which was then inverted several times  12:38- using a 10mL graduated cylinder, 10mL ethanol was measured out and added to test tube 3, which was then inverted several times  12:39- all three test tubes were inverted again  12:41- vial 1 was added to test tube 1. Parafilm was added and the test tube was inverted  12:42- vial 2 was added to test tube 2. Parafilm was added and the test tube was inverted  12:43- vial 3 was added to test tube 3. Parafilm was added and the test tube was inverted  12:45- about 200 microliters of each sample was placed into NMR tubes. The original test tubes had parafilm replaced around the cap.  12:47- 1 mL CDCl3 was added to each NMR tube  12:55- Sample 1 (test tube 1 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_1.dx” <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;"> 13:06- Sample 2 (test tube 2 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_2.dx” <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;"> 13:09- Sample 3 (test tube 3 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_3.dx” <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;"> 13:41- Sample 1 (test tube 1 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_1-2.dx” <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;"> 13:46- Sample 2 (test tube 2 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_2-2.dx” <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;"> 13:50- Sample 3 (test tube 3 contents and CDCl3) was ran with the 500 Hz NMR and was saved as “minEXP278_reaction_mixture_3-2.dx”
 * <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">12:06- Room temperature was 20C. Three 20mL test tubes were labeled 1 through 3.

<span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">2102-02-29 <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">12:45 Took overnight samples of all 3 on the 500MHz NMR. <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">minEXP278_reaction_mixture_1-3.dx <span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">minEXP278_reaction_mixture_2-3.dx

<span style="background-color: #ffffff; color: #000000; display: block; font-family: times new roman,new york,times,serif; font-size: 16px;">minEXP278_reaction_mixture_3-3.dx ||