All+Reactions



=List of all experiments=

NOTE: All solubility experiments by the Bradley group past this point are recorded on the ONS challenge wiki.
EXP286 Synthesis of aldol condensation product of phenanthrene-9-carboxaldehyde and acetone in methanol using NaOH as the catalyst. -**Matthew McBride** EXP285 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - **Matthew McBride** EXP284 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - **Matthew McBride** EXP283 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - **Matthew McBride** EXP282 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as catalyst. - **Matthew McBride** EXP281 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - **Matthew McBride** Exp280 Synthesis of benzalaniline in ethanol to prepare enough for solubility studies. Exp279 Synthesis of benzalaniline in ethanol to test the effect of the ratio of aldehyde to amine- **Mark** Exp278 Synthesis of benzalaniline in ethanol to test the effect of the ratio of aldehyde to amine- **Mark** Exp277 Synthesis of Benzalaniline in Methanol at 0.2M to test kinetic reaction rate- **Mark** Exp276 Synthesis of benzalaniline in ethanol at 0.2M and to test amine effect of concentrations - **Mark** Exp275 Observing the hydrolysis of benzalaniline in 90/10(vol) methanol/water solution - **Evan** Exp274 Synthesis of benzalaniline in methanol at 2M and recrystallization in ethanol to test yield predictions - **Evan** Exp273 Observing the hydrolysis of benzalaniline in 90/10(vol) ethanol/water solution **- Evan** Exp272 Determination of the melting point of cyclobutylamine - **Evan** Exp271 Synthesis of benzalaniline in trifluoroethanol, n-hexane and isopropanol **- Evan** Exp270 Recovery of benzalaniline from ONSexp213 **- Evan** Exp269 Synthesis of 3 imines from salicylaldehyde, 4-(dimethylamino)benzaldehyde and p-anisaldehyde with aniline. **- Evan** Exp268 Synthesis of an imine from vanillin and aniline - **Evan** Exp267 Determination of the melting point of benzylamine **JCB** Exp266 Determination of the melting point of 4-benzyltoluene - **Evan** Exp265 Determination of the melting point of benzylamine - **Evan** Exp264 Synthesis of Ugi 233 and Ugi 234 Repeat **- David** @Exp263 Synthesis of benzalaniline at 2M concentration in ethanol - **Evan** Exp262 Synthesis of four imines from vanillin, //p//-chlorobenzaldehyde, aniline and //o//-chloroaniline **- Evan** Exp261 Synthesis of an imine from benzaldehyde and aniline - **Evan** Exp260 Synthesis of Ugi products from formaldehyde, methylamine, formic acid and n-butylisocyanide and t-butylisocyanide in methanol- **Khalid** Exp259 Ugi synthesis of UCExp064C - **Khalid** Exp258 Ugi synthesis of the precursor of praziquantel - **Khalid** Exp257 Synthesis of UC176C in ethyl acetate - **Khalid** Exp256 Synthesis of UC176C in benzene - **Khalid** Exp255 Synthesis of UC176C in methanol and benzene - **Khalid** Exp254 Kinetic study for the formation UC176C in methanol via a Ugi reaction - **Khalid** Exp253 Synthesis of three Ugi products UC176C in methanol - **Khalid** Exp252 Kinetic study of Ugi reaction for the formation of UC176C in benzene - **Khalid** Exp251 Synthesis of three Ugi products, UC176C, 148C and 150D - **Khalid** Exp250 Synthesis of a Ugi product in benzene - **Khalid** Exp249 Kinetic study of Ugi reaction in benzene - **Khalid** Exp248 Synthesis of methyl ester of L-tryptophan- **Khalid** Exp247 Synthesis of 10 Ugi products in THF - **Khalid** Exp246 Kinetic study of Ugi reaction in benzene - **Khalid** Exp245 Synthesis of top 20 Ugi products in methanol - **Khalid** Exp244 Synthesis of 2 Ugi products in benzene - **Marshall Moritz** Exp243 Oxidation of 1-phenylethanol with NaH -**Khalid, Marshall** Exp242 Synthesis of 10 Ugi products in benzene with phenanthrene-9-carboxaldehyde - **Marshall Moritz** Exp241 Ugi synthesis of 38 Ugi products in methanol - **Khalid** Exp240 Ugi synthesis of 12 Ugi products in THF with phenanthrene-9-carboxaldehyde - **Khalid** Exp239 Synthesis of a Ugi product in benzene with phenanthrene-9-carboxaldehyde - **Marshall Moritz** Exp238 Ugi synthesis of 44 Ugi products in THF with phenanthrene-9-carboxaldehyde as aldehyde component - **Khalid**, **Cedric** Exp237 Ugi synthesis of a Ugi product in methanol and THF with phenanthrene-9-carboxaldehyde - **Khalid** Exp236 Ugi synthesis of 28 Ugi products in methanol - **Khalid** Exp235 Ugi synthesis of two Ugi products in methanol - **Khalid, Jenna** Exp234 Ugi synthesis of ten Ugi products in methanol ([|Ugi Reaction Blog#002]) - **David** Exp233 Ugi synthesis of six Ugi products in methanol ([|Ugi Reaction Blog#001]) - **David** Exp232 Ugi synthesis of 75 Ugi products in methanol - **Khalid** Exp231 Ugi synthesis of nine Ugi products from the top 20 list of Sortase inhibitors - **Khalid** Exp230 Ugi synthesis of four Ugi products in eight solvents at three concentrations - **David** Exp229 Ugi synthesis of two new Ugi products in methanol - **David** Exp228 Ugi synthesis of seven Ugi products six of them were in the top 20 list of Sortase inhibitors - **Khalid** Exp227 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid - **Khalid** Exp226 Ugi synthesis of eight Ugi products with1-pyrenebutyric acid - **David** Exp225 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- **Khalid** Exp224 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- **Khalid** Exp223 Ugi synthesis of previously made 62E - **David** Exp222 Effect of solvent and conc on few Ugi reactions- **Khalid** Exp221 Effect of solvent and conc on few Ugi reactions - **Khalid** Exp220 Effect of solvent and conc on few Ugi reactions - **Khalid** Exp219 Three Ugi reactions involving 4-pyrenebutanoic acid in a bisolvent system (methanol/THF) - **Khalid** Exp218 To test if deuterated methanol, acetone, chloroform and benzene can be distinguished by smell - **Khalid** Exp217 Effect of THF as solvent on for 4 Ugi reaction, Effect of DMSO as a solvent on a Ugi reaction. - **Khalid** Exp216 Ugi synthesis of ten previously made and three new Ugi products. - **Khalid** Exp215 Ugi synthesis of nine Ugi products. - **Khalid** Exp214 Ugi synthesis of previously made 150D using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butylisocyanide - **Khalid** Exp213 Solubility of 4-chlorobenzaldehyde in chloroform and methanol by UV spectroscopy - **Khalid** EXP212 Solubility measurements of p-nitrobenzaldehyde in different solvents. **Tim** EXP211 Solubility estimation by UV-VIS **Khalid** EXP210 Solubility estimation in methanol and ethanol **Khalid** EXP209 Determination of the time parameter for chloroform containing solutions in speedvac. **Khalid/Tim** EXP208 Solubility measurements of 9 aldehydes in 6 different solvents. **Khalid/Tim** EXP207 Solubility measurements of boc-gly, vanillin and other compounds in methanol, ethanol and THF **JCB** Exp206 Purification of the [|ugi product] - **Khalid** Exp205 Solubilities of 10 aldehydes in methanol -**Tim and Khalid** Exp204 Determination of solubility of Ugi adduct (99C) in Methanol, Ethanol, Acetonitrile, Tetrahydrofuran, Acetone, Hexane, Chloroform, and Distilled Water - **Cedric and Aneta** Exp203 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp202 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp201 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp200 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide (verified by TomO) - **Khalid** Exp199 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide (verified by TomO) - **Khalid** Exp198 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp197 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp196 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp195 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp194 //**missing**// Exp193 //**missing**// Exp192 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and //tert//-butyl isocyanide - **Khalid** Exp191 Repeat of Exp189 - **Khalid** Exp190 42 Ugi reactions on Minimapper -Trial 2 - **Khalid** Exp189 Ugi reaction optimization using MiniMapper - Trial 1 - **Khalid** Exp188 Ugi synthesis- Effect of Concentration - **Khalid** Exp187Ugi synthesis- Effect of Concentration - **Khalid** Exp186 Ugi synthesis (V2 Rank 83) using benzaldehyde, aniline, 1-pyrenebutyric acid and n-butylisocyanide-**Emily** Exp185 Ugi synthesis- Effect of Concentration - **Khalid** Exp184 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- **Emily** Exp183 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- **Emily** Exp182 Ugi synthesis (V1 Rank 28) using heptylamine, phenanthrene-9-carboxaldehyde, furoic acid and n-butyl isocyanide- **Emily** Exp181 Synthesis of compounds ranked 55-124 from library DEXP014-V2B **Khalid** Exp180 Ugi synthesis (V1 Rank 40) using heptylamine, phenanthrene-9-carboxaldehyde, acetic acid and n-butyl isocyanide- **Shannon** Exp179 Ugi synthesis (V1 Rank 44) using aniline, phenanthrene-9-carboxaldehyde, 4-chlorophenyl acetic acid and t-butyl isocyanide- **Shannon** Exp178 Ugi synthesis (V1 Rank 29) using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- **Shannon** Exp177 Ugi synthesis (V1 Rank 38) using propylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- **Shannon** Exp176 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- **Emily/ Khalid** Exp175 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- **Emily/Khalid** Exp174 Synthesis of compounds ranked 31-54 (except 32,37) from library DEXP014-V2B **Khalid** Exp173 Synthesis of compounds ranked 13-29 (except 23) from library DEXP014-V2B **Khalid** Exp172 (**aborted**) Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-**Lauren/Tim (repeat of Exp168)** Exp171 Synthesis of compounds ranked 1-12 from library DEXP014-V2B **Khalid** Exp170 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- **Emily** Exp169 !! Ugi synthesis using phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid, cyclohexylamine, and t-butyl isocyanide.-**Tim** Exp168 !! Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-**Tim** Exp167-!! Ugi synthesis using propylamine, phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid and n-butyl isocyanide- **Tim.** Exp166 !! Plasmodium falciparum inhibition results for 2 Ugi products **Jiri** Exp165 !! Falcipain-2 inhibition results for 2 Ugi products **Jiri** Exp164 Ugi synthesis using aniline, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- **Emily/Shannon** Exp163 !! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- **Tim** (repeat of Exp161) Exp162 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide (Repeat of Exp157)- **Shannon** Exp161-!! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- **Tim** Exp160 !! synthesis using phenanthrene-9-carboxaldehyde, furfurylamine, 3,4-dihydroxyphenyl acetic acid and n-butyl isocyanide- **Emily** Exp159 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- **Emily** Exp158 Ugi synthesis using 4-chlorobenzaldehyde, 5-methylfurfurylamine, salicylic acid and tosylmethyl isocyanide- **Emily** Exp157 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide- **Shannon** Exp156 Ugi synthesis using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butyl isocyanide- **Emily** Exp155 Ugi synthesis using benzaldehyde, 5-methyl-2-furylmethylamine, 3-(4-methoxyphenyl) propanioc acid, and t-butyl isocyanide- **Tim/Emily** Exp154 Three attempts of Ugi synthesis- **Shannon** Exp153 One attempt of Ugi synthesis -**Mitesh** Exp151 One attempt of Ugi synthesis- **Mitesh** Exp150 Ugi synthesis with Benzylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and tert-butyl isocyanide- **Emily** / **Khalid** Exp149 ugi synthesis using phenanthrene -9- carboxaldehyde, hexylamine, benzoic acid and n-butylisocyanide., **Aneh/ Khalid** Exp148 Ugi synthesis with Heptylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and //tert-//butyl isonitrile - **Emily / Khalid** Exp147 Four attempts of Ugi synthesis - **Mitesh/Rikesh** Exp146 Two attempts of Ugi synthesis - **Rikesh/Mitesh** Exp144 Three attempts of Ugi synthesis - **Rikesh/Mitesh** Exp143 Five attempts of Ugi synthesis - **Emily** Exp142 Two attempts of Ugi synthesis - **Rikesh**/**Mitesh** Exp141 Two attempts of Ugi synthesis - **Rikesh/Mitesh** Exp140 Two attempts of Ugi synthesis - **Emily/ Khalid** Exp139 Ten attempts of Ugi synthesis-**aneh** Exp138 Three attempts of Ugi synthesis - **Shannon** Exp137 Eight attempts of Ugi synthesis - **Anett, Rikesh, Mitesh, Khalid** Exp136 Ugi synthesis using o-vanillin, benzylamine, Boc-Trp-OH, and n-pentylisocyanide - **Mitesh/Rikesh** Exp135 Ugi synthesis using o-vanillin, hexylamine, Boc-Trp-OH, and benzyl isocyanide - **Rikesh** Exp134 Four attempts of Ugi synthesis - **Rikesh** Exp133 Synthesis of N-benzyl-N-(2-furylmethyl)acetamide - **Khalid** Exp132 Synthesis of N-benzyl-N-[(5-methyl-2-furyl)methyl]acetamide - **Khalid** Exp131 Nine Attempts of Ugi synthesis - **Rikesh** Exp130 Five Attempts of Ugi synthesis - **Rikesh** Exp129 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - **Jessica****/ Khalid** Exp128 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - **Jessica****/ Khalid** Exp127 Test for the stability of the furan ring of 109C Ugi adduct in TFA - **Jessica****/ Khalid** Exp126 Five attempts of Ugi synthesis - **Jessica** Exp125 Three attempts of Ugi synthesis - **Jessica** Exp124 Two attempts of Ugi synthesis - **Khalid** Exp123 Ugi synthesis using furfuylamine, o-vanillin, Boc-Tryptophan, and n-butyl isocyanide - **Jessica** Exp122 Ugi synthesis using methylamine, o-tolualdehyde, acetic acid, and //p//-toluenesulfonylmethyl isocyanide - **Jessica** Exp121 Ugi synthesis using //o//-Vanillin, 5-methyl furfurylamine Boc-tryptophan and 1-pentylisocyanide- **Khalid** Exp120 Ugi synthesis using //o//-Vanillin, furfurylamine Boc-tryptophan and 1-pentylisocyanide- **Khalid** Exp119 Two attempts of Ugi synthesis - **Jessica/ Khalid** Exp118 Purify propionaldehyde by distillation - **Khalid** Exp117 Monitor Ugi synthesis using propionaldehyde, methylamine, acetic acid and //tert//-butyl isocyanide by NMR - **Khalid** Exp116 Four attempts of Ugi synthesis - **Khalid** Exp115 Monitor Ugi synthesis using furfural, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid by NMR - **Khalid** Exp114 Ugi synthesis using furfuraldehyde, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid - **Khalid** Exp113 Ugi synthesis using Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, and Boc-glycine - **Jessica****/ Khalid** Exp112 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - **Khalid / Jessica** Exp111 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - **Khalid / Jessica** Exp110 Reaction of the Ugi product 108C with 50% TFA in CDCl3 (prolonged exposure) - **Khalid** / **Jessica** Exp109 Ugi synthesis using 5-(Trifluoromethyl)-2-furylmethylamine, benzaldehyde, benzylisocyanide and boc-glycine - **Khalid** Exp108 Ugi synthesis using furfurylamine, benzaldehyde, benzylisocyanide and boc-glycine - **Khalid** Exp107 Tert-butylation of furfurylamine with t-butanol and Amberlyst 15(H) in CDCl3 at room temperature **- Khalid** Exp106 Ugi synthesis using 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide and Boc-Gly-OH - **Sean** Exp105 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide**-Khalid** Exp104 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp103 Synthesis of the acetamide of furfurylamine -**Khalid** Exp102 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide**-Khalid** Exp101 Reaction of the Ugi product 99C with 50% TFA in CDCl3 (prolonged exposure) - **Khalid** Exp100 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp099 Ugi synthesis using furfurylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp098 Reaction of the Ugi product 64C with 50% TFA in CDCl3 (prolonged exposure) **- Khalid** Exp097 Reaction of the Ugi product 86B with 50% TFA in CDCl3 (prolonged exposure) - **Khalid** Exp096 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp095 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp094 3,4-Dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Glycine, t-Butyl isocyanide (CHCl3 for imine, MeOH for rxn) - **Sean** Exp093 Ugi synthesis using aniline, benzophenone, tert-butylisocyanide and boc-glycine - **Khalid** Exp092 Test for the stability of the furan ring of amide of BocGlycine and 5MFA in 50% TFA - **Khalid** Exp091 Reaction of the Ugi product 62E with 50% TFA in CDCl3. **- Khalid** Exp090 Reaction of the Ugi product 62E with 10% TFA in CDCl3 - **Alicia** Exp089 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - **Khalid** Exp088 Synthesis of an amide of Boc Glycine and 5-methylfurfurylamine in methanol-d4- **Khalid** *Exp087 Synthesis of the Boc-deprotected amine of the Ugi product 86C**- Khalid** Exp086 Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, Boc-glycine - **Khalid** Exp085Crotonaldehyde, Methylfurfurylamine in CDCl3 - **jgiammarco** Exp084Piperonal, Aniline, Boc-Gly-OH, Tertbutyalisocyanide in CDCl3- **jgiammarco** Exp083Crotonaldehyde, Tertbutyalamine, Boc-Gly-OH, Tertbutylisocyanide in CDCl3- **jgiammarco** Exp082 Synthesis of the Boc-deprotected amine of the Ugi product(64C-2) - **Khalid** Exp081 Test for the stability of the furan ring of N-[(5-methyl-2-furyl)methyl]acetamide in 10% TFA - **Khalid** Exp080 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutylisocyanide (CDCl3) -**jgiammarco** Exp079 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - **Alicia** Exp078 Synthesis of the acetamide of 5-methyl furfurylamine -**Khalid** Exp077 Piperonal, tertbutylamine, Boc-Gly-OH(CDCl3) -**jgiammarco** Exp076 Piperonal, tertbutylamine, Boc-Gly-OH (MeOH) -**jgiammarco** Exp075 Perform a MALDI MS analysis of the Ugi product 62E - **kgowens** Exp074 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - **Khalid** Exp073 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - **Khalid** Exp072 Ugi Product (diamide) Cycliztion using 10% HCl in CDCl3 - **Alicia** Exp071 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - **Khalid** Exp070 Ugi Product (diamide) Cycliztion using 50% TFA in CDCl3 - **Khalid** Exp069 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - **jgiammarco** Exp068 Reaction of Boc-Glycine with 10%TFA in CDCl3 - **Khalid** Exp067 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - **Khalid** Exp066 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - **jgiammarco** *Exp065 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - **Alicia** *Exp064 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH - **Khalid** *Exp063 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, benzyl isocyanide - **Sean** *Exp062 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - **Alicia** *Exp061 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, t-butyl isocyanide - **Sean** *Exp060 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH- **Khalid** *Exp059 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - **Alicia** Exp058 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - **jgiammarco** Exp057 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - **Sean** Exp056 Boc-Met-OH and 5-Methyl furfurylamine in MeOH-d4 - **Khalid** Exp055 Boc-Gly-OH and 5-Methyl furfurylamine in MeOH-d4 - **Khalid** Exp054 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide and final addition of Boc-Gly-OH in MeOH-d4 - **Khalid** Exp053 Boc-Gly-OH and //tert//-butyl isocyanide in MeOH-d4 - **Khalid** *Exp052 Piperonal, 5-methylfurfurylamine, BocGly-OH, //tert//-butyl isocyanide in MeOH - **Alicia** Exp051 Piperonal and //tert-//butylamine, Boc-Gly-OH and dehydration with MgSO4 in MeOH-d4 **- jgiammarco** Exp050 Boc-Gly-OH and Benzyl isocyanide in MeOH-d4 - **Khalid** Exp049 Boc-Gly-OH and 2-morpholinoethyl isocyanide in MeOH-d4 - **Khalid** Exp048 (piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH-d4) - **jgiammarco** Exp047 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - **Sean** Exp046 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in MeOH-d4) **- Khalid** *Exp045 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) **- Khalid** Exp044 Formation of the imine of Phenyl acetaldehyde and //tert-//butylamine in CDCl3- **Khalid** Exp043 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4 - **Alicia** Exp042 Formation of the imine of Phenyl acetaldehyde and //tert-//butylamine in CDCl3- **Khalid / Lin** Exp041 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4- **Alicia** Exp040 Formation of the imine of Piperonal and 5-Methyl furfurylamine in CDCl3- **Alicia** Exp039 Distillation of Phenylacetaldehyde (**39B pure**) - **Khalid / Lin** Exp038 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3 ) - **Alicia** Exp037 Distillation of Phenylacetaldehyde (contaminated)- **jgiammarco** Exp036 Preparation of N-//tert-//butylphenylacetaldimine (impure by HMR)**- Khalid** Exp035 Distillation of Phenylacetaldehyde(impure by HMR) - **Khalid** Exp034 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) - **Alicia** Exp033 Distillation of Butyraldehyde (impure by HMR) - **Alicia** Exp032 (Imine mix from Exp036, Boc-Met-OH, 2-morpholinoethylisocyanide in MeOH ) - **Khalid** Exp031 (Phenylacetaldehyde after distillation, -methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) **- jgiammarco** Exp030 (Piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH) **- Khalid** Exp029 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH then CDCl3) - **Alicia** Exp028 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in 1M LiCl/Water) - **Khalid** Exp027 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in Methanol) **-** **Khalid** Exp026 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) **Lin** EXP025 Convert adrenaline to [|DOPAL] by acid catalysis **- (2006-08-31) Khalid/Lin (pure without chromatography)** EXP024 Convert adrenaline to [|DOPAL] by acid catalysis **- Khalid/Lin** EXP023 ([|DOPAL], 5-methylfurfurylamine, N-(tert)-butoxycarbonyl)-L-methionine, and benzylisocyanide) - **Khalid (crude)** EXP022 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) **Khalid** EXP021 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) **jgiammarco** EXP020 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) **jgiammarco** EXP019 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) - **Lin** EXP018 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) **jgiammarco** EXP017 (Piperonal, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) - **Lin** [|EXP016] Convert adrenaline to [|DOPAL] using phosphoric acid - **jgiammarco** [|EXP015] Convert adrenaline to [|DOPAL] using phosphoric acid - **jgiammarco** EXP014 (Phenylacetaldehyde, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) **- Khalid** [|EXP013] Convert adrenaline to a catechol aldehyde using CH3COOH- **jgiammarco** [|EXP012] Convert adrenaline to a catechol aldehyde using H2SO4- **jgiammarco** [|EXP011] Convert adrenaline to a catechol aldehyde using H2SO4 and a benzene layer- **jgiammarco** [|EXP010] Convert adrenaline to a catechol aldehyde using H2SO4 - **jgiammarco** [|EXP009] Convert adrenaline to a catechol aldehyde using H2SO4, benzene, and water - **jgiammarco** [|EXP008] Convert adrenaline to a catechol aldehyde using H2SO4 and benzene - **jgiammarco** [|EXP007] Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - **Alicia** [|EXP006] (Phenylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) **- Khalid** [|EXP005] Synthesis of 3,4-dihydroxyphenylacetaldehyde from adrenaline -**jgiammarco** [|EXP004] Convert adrenaline to a catechol aldehyde using CH3COOH, H2SO4, and water - **Brett** [|EXP003] (Phehylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) - **Brett/Alicia/jgiammarco** [|EXP002] Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - **jgiammarco** [|EXP001] Convert adrenaline to a catechol aldehyde using MeOH - **Jean-Claude Bradley**


 * [|Usefulchem Table of Chemicals]**

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