Exp192

=Objective= To synthesize 48 Ugi products using five aldehydes, four amines, two acids and tert-butyl isocyanide using Mettler Toledo's MiniMapper =Procedure= The MiniMapper is mapped to dispense methanol (1.5mL) followed by each reactant (1mmol) according to the [|spreadsheet].

[|Job file]  =Results=
 * 1) 2-Furaldehyde - 1:A
 * 2) 4-triflurormethyl benzaldehyde - 2:A
 * 3) Benzaldehyde - 3:A
 * 4) crotonaldehyde - 4:A
 * 5) p-tolualdehyde -5:A
 * 6) t-butylamine : 6:A
 * 7) n-propylamine- 1:B
 * 8) benzylamine - 2:B
 * 9) 5-methylfurfurylamine 3:B
 * 10) 1-hexanoic acid - 4:B
 * 11) 1-butanoic acid - 5:B
 * 12) t-butylisocyanide - 6:B

=Discussion=

=Conclusion= The results are not meaningful because the liquid handler was not properly programmed.

Log
[|Log file] 18:00 Removed the miniblock from the mapper transferred on to the shaker (600 rpm) //**when was it removed from the shaker?**//
 * 2008-06-27**