Exp277

Purpose
To synthesize Benzalaniline in Methanol at 0.2M to test kinetic reaction rate

Results
[|Mass And Yield Calculations] [|NMR of Reaction Mixture]

Discusion
The NMR performed on the 500MHz machine clearly shows the peaks for both the desired Imine as well as the acid product.

Log
12:15 Added 0.622g of 4-chlorobenzaldehyde to a 20 test-tube. 12:20 Added 0.460g of analine to the test tube. Mixed and transfered a small sample to a NMR tube. 12:40 Took first NMR sample on the 300MHz NMR, was not able to lock the sample. 13:00 Took second NMR sample, still no lock. 13:20 Took third NMR sample, still no lock. 13:40 Took forth and final sample, still no lock.
 * 2012-02-15**

Took an NMR of the reaction mixture on the 500MHz NMR in CDCl3, and had no trouble locking the sample.
 * 2012-02-20**