Exp275

=Researcher= Evan Curtin =Objective= To observe the hydrolysis of benzalaniline in methanol using a deuterated solvent (methanol-d4). =Procedure= =Results= Volume Calculations Sheet =Discussion= =Conclusion= =Log=

2011-08-18
15:30 - Weighed out benzalaniline and transferred to an NMR tube. 15:34 - Mixed ~1mL Methanol with about 0.3-0.5mL CD3OD, added 0.9mL (measured with a syringe) of this mixture to the benzalaniline. 16:01 - Took HNMR 1 of methanol/benzalaniline solution using 300MHz varian NMR. 16:04 - Added 0.1mL H2O to the NMR tube. Precipitate formed immediately upon addition, but dissolved after mixing. 16:09 - Took HNMR 2 16:14 - Took HNMR 3 16:24 - Took HNMR 4 16:44 - Took HNMR 5 17:24 - Took HNMR 6